Synthesis of monosubstituted thioureas by vapour digestion and mechanochemical amination of thiocarbamoyl benzotriazoles
Author:
Affiliation:
1. Division of Organic Chemistry and Biochemistry
2. Ruđer Bošković Institute
3. 10 000 Zagreb
4. Croatia
5. Diamond Light Source Ltd
6. Harwell Science and Innovation Campus
7. OX11 0DE Didcot
8. UK
Abstract
N-monosubstituted thioureas have been rapidly accessed from thiocarbamoyl benzotriazoles by ammonia vapour digestion and solvent-free mechanochemical milling in near-quantitative yields.
Funder
Hrvatska Zaklada za Znanost
Publisher
Royal Society of Chemistry (RSC)
Subject
Pollution,Environmental Chemistry
Link
http://pubs.rsc.org/en/content/articlepdf/2016/GC/C6GC00089D
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