Synthesis by extrusion: continuous, large-scale preparation of MOFs using little or no solvent

Author:

Crawford Deborah1234,Casaban José564,Haydon Robert1234,Giri Nicola1234,McNally Tony789104,James Stuart L.12345

Affiliation:

1. School of Chemistry and Chemical Engineering

2. Queen's University Belfast

3. Belfast

4. UK

5. MOF Technologies Ltd

6. Belfast BT7 1NF

7. IINM

8. WMG

9. University of Warwick

10. Coventry

Abstract

Continuous flow mechanochemical and melt-phase synthesis at kg h−1 rates from solid reagents and either no solvent, or only minimal solvent, is reported.

Funder

Engineering and Physical Sciences Research Council

Publisher

Royal Society of Chemistry (RSC)

Subject

General Chemistry

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