Fast and accurate diffusion NMR acquisition in continuous flow-Reference-Cited by-同舟云学术

Fast and accurate diffusion NMR acquisition in continuous flow

Published:2022 Issue:59 Volume:58 Page:8242-8245
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Thomlinson Isabel A.¹²³^ORCID,Davidson Matthew G.¹³,Lyall Catherine L.²³^ORCID,Lowe John P.²³^ORCID,Hintermair Ulrich¹²³^ORCID

Affiliation:

1. Centre for Sustainable and Circular Technologies, University of Bath, Claverton Down, Bath BA2 7AY, UK

2. Dynamic Reaction Monitoring Facility, University of Bath, Claverton Down, Bath BA2 7AY, UK

3. Department of Chemistry, University of Bath, Claverton Down, Bath BA2 7AY, UK

Abstract

Measuring molecular diffusion in a moving sample? Possible through convection compensation with appropriate acquisition parameters and a low pulsation pump or a simple correction factor!

Funder

Royal Society

Engineering and Physical Sciences Research Council

University of Bath

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2022/CC/D2CC03054C

Reference23 articles.

1. Practical aspects of real-time reaction monitoring using multi-nuclear high resolution FlowNMR spectroscopy

2. Insight into catalyst speciation and hydrogen co-evolution during enantioselective formic acid-driven transfer hydrogenation with bifunctional ruthenium complexes from multi-technique operando reaction monitoring

3. Mechanistic Study of In Situ Generation and Use of Methanesulfonyl Azide as a Diazo Transfer Reagent with Real-Time Monitoring by FlowNMR

4. Online monitoring of a photocatalytic reaction by real-time high resolution FlowNMR spectroscopy

5. Multi-nuclear, high-pressure, operando FlowNMR spectroscopic study of Rh/PPh3 – catalysed hydroformylation of 1-hexene

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