Use of Doehlert design in the optimization of extraction conditions in the determination of organochlorine pesticides in bovine milk samples by HS-SPME
Author:
Affiliation:
1. Departamento de Química
2. Universidade Federal de Santa Catarina
3. Florianópolis 88040-900, Brazil
Abstract
The extraction of pesticides lindane, heptachlor, aldrin, dieldrin and endrin from milk by HS-SPME was investigated followed by separation/detection of these compounds by GC-ECD.
Publisher
Royal Society of Chemistry (RSC)
Subject
General Engineering,General Chemical Engineering,Analytical Chemistry
Link
http://pubs.rsc.org/en/content/articlepdf/2014/AY/C4AY00202D
Reference24 articles.
1. Solid-phase microextraction as a clean-up and preconcentration procedure for organochlorine pesticides determination in fish tissue by gas chromatography with electron capture detection
2. In vivo and in vitro effects of the organochlorine pesticides DDT, TCPM, methoxychlor, and lindane on the female reproductive tract of mammals: A review
3. Development of a solid-phase microextraction gas chromatography with microelectron-capture detection method for a multiresidue analysis of pesticides in bovine milk
4. Analytical methods applied to the determination of pesticide residues in foods of animal origin. A review of the past two decades
5. Optimisation of solid-phase microextraction coupled to HPLC-UV for the determination of organochlorine pesticides and their metabolites in environmental liquid samples
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