Abstract
A new data acquisition system forin situtime-resolved three-dimensional reciprocal space mapping is reported. The system is based on a programmable microcontroller for generating a functional low-voltage signal, a pixel area detector serving as a master clock and a high-voltage amplifier. Both Bragg and diffuse scattering can be mapped in a large volume of reciprocal space under an alternating electric field of a pre-programmed shape. The system has been tested at the Swiss–Norwegian Beamline BM01 of the European Synchrotron by measuring the electric field dependence of diffuse X-ray scattering from a functional perovskite-based ferroelectric single crystal.
Funder
Bundesministerium für Bildung und Forschung
Russian Science Foundation
Publisher
International Union of Crystallography (IUCr)
Subject
General Biochemistry, Genetics and Molecular Biology
Reference9 articles.
1. Choe, H., Gorfman, S., Heidbrink, S., Pietsch, U., Vogt, M., Winter, J. & Ziolkowski, M. (2017). IEEE Trans. Nucl. Sci. PP(99), 1.
2. Combining high time and angular resolutions: time-resolved X-ray powder diffraction using a multi-channel analyser detector
3. A new multipurpose diffractometer PILATUS@SNBL
4. Sub-microsecond X-ray crystallography: techniques, challenges, and applications for materials science
5. Crystallography under External Electric Field
Cited by
11 articles.
订阅此论文施引文献
订阅此论文施引文献,注册后可以免费订阅5篇论文的施引文献,订阅后可以查看论文全部施引文献