Development of a Scalable Process for the Insecticidal Candidate Tyclopyrazoflor. Part 2. Fit-for-Purpose Optimization of the Route to Tyclopyrazoflor Featuring [3 + 2] Cyclization of 3-Hydrazinopyridine·2HCl and Methyl Acrylate-Reference-Cited by-同舟云学术

Development of a Scalable Process for the Insecticidal Candidate Tyclopyrazoflor. Part 2. Fit-for-Purpose Optimization of the Route to Tyclopyrazoflor Featuring [3 + 2] Cyclization of 3-Hydrazinopyridine·2HCl and Methyl Acrylate

Published:2019-07-01 Issue:10 Volume:23 Page:2133-2141
ISSN:1083-6160
Container-title:Organic Process Research & Development
language:en
Short-container-title:Org. Process Res. Dev.

Author:

Yang Qiang¹^ORCID,Li Xiaoyong¹^ORCID,Lorsbach Beth A.²,Muhuhi Joseck M.¹,Roth Gary A.¹,Gray Kaitlyn¹^ORCID,Podhorez David E.¹

Affiliation:

1. Product Design & Process R&D, Corteva Agriscience, 9330 Zionsville Road, Indianapolis, Indiana 46268, United States

2. Discovery Chemistry, Corteva Agriscience, 9330 Zionsville Road, Indianapolis, Indiana 46268, United States

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Physical and Theoretical Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/acs.oprd.9b00128

Reference20 articles.

1. Asymmetric Fluorination Approach to the Scalable Synthesis of a SYK Inhibitor

2. Development of the Commercial Route for the Manufacture of a 5-Lipoxygenase Inhibitor PF-04191834

3. An Automated Intermittent Flow Approach to Continuous Suzuki Coupling

4. Early Development Scale-Up of a Structurally-Challenging 5-Lipoxygenase Activating Protein (FLAP) Inhibitor

5. Synthesis of the Hydrazinyl Pyridine Intermediate: Phase-Appropriate Delivery

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