Author:
Goodwin HA,Kucharski ES,White AH
Abstract
The crystal structure of
the title compound [Fe(mphen)3] (BPh4)2
a high-spin derivative of iron(II), has been determined by a single crystal
X-ray diffraction study at 295 K, being refined to a residual of 0.055 for 4079
'observed' reflections. Crystals are monoclinic P 21/c, a 12.326(8), b 15.387(8), c 3679(3) �,
β 98.80(6)�, Z 4. The metal atom environment is considerably distorted
from ideal D3 point symmetry; Fe-N distances range from 2.143(5) to
2.294(4)�.
Cited by
31 articles.
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