High-Throughput Analyses of Microplastic Samples Using Fourier Transform Infrared and Raman Spectrometry

Author:

Brandt Josef12ORCID,Bittrich Lars13,Fischer Franziska1,Kanaki Elisavet1ORCID,Tagg Alexander4,Lenz Robin4ORCID,Labrenz Matthias4,Brandes Elke5,Fischer Dieter1,Eichhorn Klaus-Jochen1

Affiliation:

1. Leibniz-Institut für Polymerforschung Dresden e.V., Dresden, Germany

2. Department of Marine Sciences, University of Gothenburg, Fiskebäckskil, Sweden

3. Complex Fiber Structures GmbH, Dresden, Germany

4. Leibniz-Institut für Ostseeforschung Warnemünde, Rostock, Germany

5. Johann Heinrich von Thünen-Institut, Braunschweig, Germany

Abstract

Determining microplastics in environmental samples quickly and reliably is a challenging task. With a largely automated combination of optical particle analysis, Fourier transform infrared (FT-IR), and Raman microscopy along with spectral database search, particle sizes, particle size distributions, and the type of polymer including particle color can be determined. We present a self-developed, open-source software package for realizing a particle analysis approach with both Raman and FT-IR microspectroscopy. Our software GEPARD (Gepard Enabled PARticle Detection) allows for acquiring an optical image, then detects particles and uses this information to steer the spectroscopic measurement. This ultimately results in a multitude of possibilities for efficiently reviewing, correcting, and reporting all obtained results.

Publisher

SAGE Publications

Subject

Spectroscopy,Instrumentation

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