1. Department of Orthodontics, materials, Institute of Dental Science, Matsumoto Dental College, 1780 Gohbara Hirooka, Shiojiri, Nagano 399-07, Japan
2. Department of Biomaterials, Institute of Dental Science, Matsumoto Dental College, 1780 Gohbara Hirooka, Shiojiri, Nagano 399-07, Japan
3. Department of Orthodontics, Institute of Dental Science, Matsumoto Dental College, 1780 Gohbara Hirooka, Shiojiri, Nagano 399-07, Japan
4. Dental Materials, Indiana University School of Dentistry, Indianapolis, Indiana 46202, USA