Medium-sized Cyclophanes. Part 72. Synthesis and Structures of 9-Methoxy(1,4)Naphthaleno[3.3]Metacyclophane-2,11-Diones-Reference-Cited by-同舟云学术

Medium-sized Cyclophanes. Part 72. Synthesis and Structures of 9-Methoxy(1,4)Naphthaleno[3.3]Metacyclophane-2,11-Diones

Published:2006-09 Issue:9 Volume:2006 Page:593-595
ISSN:1747-5198
Container-title:Journal of Chemical Research
language:en
Short-container-title:Journal of Chemical Research

Author:

Yamato Takehiko¹,Okabe Ryo¹,Miyamoto Shinpei¹,Miyazaki Minoru¹

Affiliation:

1. Department of Applied Chemistry, Faculty of Science and Engineering, Saga University, Honjo-machi 1, Saga-shi, Saga 840-8502, Japan

Abstract

Syn- and anti-9-Methoxy(1,4)naphthaleno[3.3]MCP-2,11-diones (4) are obtained by the coupling reaction of 2,6-bis[2-cyano-2-(toluenesulfony)ethyl]anisoles (2) and 1,4-bis(bromomethyl)naphthalene (3) in dimethylformamide (DMF) with an excess of sodium hydride.

Publisher

SAGE Publications

Subject

General Chemistry

Link

http://journals.sagepub.com/doi/pdf/10.3184/030823406778521509

Reference13 articles.

1. Medium-size Cyclophanes, 71. Synthesis, Structures and Photo-Induced Cyclisation of 1,2-Diphenyl[2.n]Metacyclophan-1-Enes

2. NMR studies of cyclophanes

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