Synthesis of Bishomobenzoctamine 2-(9,10-Dihydro-9,10-Propanoanthracen-9-yl)-N-Methylethanamine-Reference-Cited by-同舟云学术

Synthesis of Bishomobenzoctamine 2-(9,10-Dihydro-9,10-Propanoanthracen-9-yl)-N-Methylethanamine

Published:2010-05 Issue:5 Volume:34 Page:241-242
ISSN:1747-5198
Container-title:Journal of Chemical Research
language:en
Short-container-title:Journal of Chemical Research

Author:

Karama Usama¹,Al-Saidey Adel¹,Almansour Abdel Rahman¹

Affiliation:

1. Department of Chemistry, College of Science, King Saud University, PO Box 2455, Riyadh - 11451, Saudi Arabia

Abstract

Tetracyclic bishomobenzoctamine as a homologue of benzoctamine 1 was synthesised. The key intermediate 9-(prop-2-en-1-yl)-9,10-dihydro-9,10-propanoanthracen-12-one was successfully synthesised via [3+4] cycloaddition of tetrabromoacetone on 9-allylanthracene by using ultrasonication at 15–20 °C followed by debromination.

Publisher

SAGE Publications

Subject

General Chemistry

Link

http://journals.sagepub.com/doi/pdf/10.3184/030823410X12715108891565

Reference6 articles.

1. Synthese und Eigenschaften von 1-Aminoalkyl-dibenzo[b,e]bicyclo[2.2.2]octadienen

2. Improved procedure for the generation of allyl cations from simple dibromo ketones. Change of mechanism on reaction with triethyl borate amd zinc. Cycloadditions to conjugated dienes.

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1. Synthesis of [9, 10-dihydro-9-(4-methylaminobutyl)-9, 10-propanoanthracene] using Diels–Alder cycloaddition;Journal of Saudi Chemical Society;2016-07

2. Substituent Effects on Regioselectivity of the Diels-Alder Reactions: Reactions of 10-Allyl-1,8-dichloroanthracene with 2-Chloroacrylonitrile, 1-Cyanovinyl Acetate and Phenyl Vinyl Sulfone;Journal of Chemistry;2016

3. 11-Hydroxy-9-(prop-2-en-1-yl)-9,10-dihydro-9,10-propanoanthracen-12-one;Acta Crystallographica Section E Structure Reports Online;2011-08-27

4. ChemInform Abstract: Synthesis of Bishomobenzoctamine 2-(9,10-Dihydro-9,10-propanoanthracen-9-yl)-N-methylethanamine (IX);ChemInform;2010-09-30