Affiliation:
1. Laboratori de l’Agncia de Salut Pblica de Barcelona, Edifici Peracamps, Avinguda Drassanes 13-15, 08001 Barcelona, Spain
Abstract
Abstract
A method was developed for the extraction of stanozolol, taleranol, zeranol, hexestrol, dienestrol, ethynylestradiol, diethylstilbestrol, and trenbolone from animal urine. The analytes were extracted from the matrix by enzymatic hydrolysis, solid-phase extraction, and liquidliquid extraction. Detection and quantitation were performed on a high-performance liquid chromatography system coupled to a triple quadrupole mass spectrometer. The identification criteria met the European Union regulations. Validation of this method established a decision limit between 0.2 and 0.9 μg/L and a detection capability between 0.3 and 1.0 μg/L, depending on the analyte.
Publisher
Oxford University Press (OUP)
Subject
Pharmacology,Agronomy and Crop Science,Environmental Chemistry,Food Science,Analytical Chemistry
Cited by
14 articles.
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