Microstructure of LaNi5 Base Nanopowders Produced by High Energy Ball Milling

Author:

Kusiński Jan1,Kowalski K.2,Kac Sławomir2,Matteazzi P.3,Krebs M.4,Morgiel Jerzy5,Cochet S.6

Affiliation:

1. AGH University of Science and Technology

2. AGH-University of Science and Technology

3. MBN Nanomaterialia

4. Varta Microbattery

5. Polish Academy of Sciences

6. Fraunhofer-Institute für Silicatforschung

Abstract

LaNi5 nano-powders with additions of Ce, Mn, Co (high and low content of cobalt) and Al were obtained by means of MBN technology, based on the high energy ball milling with different energy and protective atmosphere (Ar or H2). The microstructure and composition of all prepared nano-powders were investigated using the TEM/HRTEM, SEM/EDS, XRD and XPS techniques. Research showed that used technology allowed to produce materials distinguished by a fine and homogeneous chemical distribution of elements and an "ultrafine" (the nanometric size) crystalline structure. The results were then related to the preparation conditions.

Publisher

Trans Tech Publications, Ltd.

Subject

Condensed Matter Physics,General Materials Science,Atomic and Molecular Physics, and Optics

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