Abstract
Using maleic anhydride, benzyl alcohol and methanol as raw materials, a new preservative benzyl methyl fumarate containing α, β-unsaturated carbonyl structure was prepared. Based on the single factor experiment, the results of orthogonal test showed that the optimal conditions for the reaction was 4 h time, temperature at 65 °C, and with molar ratio of fumarate acid to methanol at 1:5. The production rate was 65.53%.
Publisher
Trans Tech Publications, Ltd.
Reference5 articles.
1. Z.F. Fang, S.X. Yu and R.M. Wen: Industry catalysis. Vol. 13 (2005), pp.46-48 (In Chinese).
2. C.N. Huhtanen: Journal of Food Science. Vol. 48 (1983), pp.1574-1575.
3. C.N. Huhtanen, H. Trenchard, C.M. Mccaffrey: Journal of Food Protection. Vol. 48 (1985), pp.570-573.
4. M. Dymicky, M. Bencivengo, R.L. Buchanan: Applied and Environmental Microbiology. Vol. 53 (1987), pp.110-113.
5. Y. Zhan, C. Zheng: Guangzhou Chemical Industry. Vol. 33 (2005), pp.21-23 (In Chinese).