Design, calibration, and performance of a uniaxial pressure cell for neutron scattering studies of quantum magnetism

Author:

Sandberg L. Ø.1,Haubro M. L.12ORCID,Krighaar K. M. L.1ORCID,Edberg R.3ORCID,Fjellvåg I. M. B.4,Guthrie M.567ORCID,Holmes A. T.5ORCID,Mangin-Thro L.8ORCID,Wildes A.8ORCID,Henelius P.39,Lefmann K.1ORCID,Deen P. P.110ORCID

Affiliation:

1. Niels Bohr Institute, University of Copenhagen 1 , Universitetsparken 5, 2100 Copenhagen Ø, Denmark

2. Department of Physics, Technical University of Denmark 2 , 2800 Kongens Lyngby, Denmark

3. Physics Department, KTH Royal Institute of Technology 3 , Stockholm, Sweden

4. Centre for Materials Science and Nanotechnology, University of Oslo 4 , 0315 Oslo, Norway

5. European Spallation Source ERIC 5 , 22363 Lund, Sweden

6. School of Physics and Astronomy and Centre for Science at Extreme Conditions, University of Edinburgh 6 , Edinburgh, Scotland

7. Neutron Scattering Division, Oak Ridge National Laboratory 7 , Oak Ridge, Tennessee 37830, USA

8. Institut Laue-Langevin 8 , 71 Avenue des Martyrs, CS 20156, 38042 Grenoble Cedex 9, France

9. Faculty of Science and Engineering, Åbo Akademi University 9 , Åbo, Finland

10. European Spallation Source ERIC 10 , Partikelgatan 224 84, Lund, Sweden

Abstract

We provide an overview of a pressure cell designed to apply uniaxial pressure to single crystals for the study, by neutron scattering techniques, of strongly correlated magnetic systems and, in particular, quantum magnets. A detailed overview of the pressure cell components, their requirements, and links to the scientific and technical specifications are presented. The pressure cell is able to accommodate a 200 mm3 single crystal that can be pressurized up to 2 GPa at cryogenic temperatures. The pressure cell is consistent with the requirements of inelastic neutron scattering and, importantly, neutron polarization analysis. A particular strength of the uniaxial pressure cell is the highly uniform and low background for a wide scattering angle of 360° horizontally and ±20° vertically. We show the performance of the uniaxial pressure cell using a relevant neutron scattering instrument, the polarized diffuse scattering instrument, D7. The experiments confirm that the cell complies with the scientific and technical requirements. This uniaxial pressure cell will provide a useful additional tool in the sample environment suite available for the study of quantum magnetism.

Funder

DanScatt

NordForsk

Publisher

AIP Publishing

Subject

Instrumentation

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