In situ uniaxial pressure cell for x-ray and neutron scattering experiments

Author:

Simutis G.12ORCID,Bollhalder A.1,Zolliker M.1ORCID,Küspert J.3ORCID,Wang Q.3ORCID,Das D.4ORCID,Van Leeuwen F.15ORCID,Ivashko O.6ORCID,Gutowski O.6,Philippe J.13ORCID,Kracht T.6ORCID,Glaevecke P.6,Adachi T.7ORCID,v. Zimmermann M.6,Van Petegem S.5ORCID,Luetkens H.4ORCID,Guguchia Z.4ORCID,Chang J.3,Sassa Y.2,Bartkowiak M.1ORCID,Janoschek M.13ORCID

Affiliation:

1. Laboratory for Neutron and Muon Instrumentation, Paul Scherrer Institut 1 , CH-5232 Villigen PSI, Switzerland

2. Department of Physics, Chalmers University of Technology 2 , SE-41296 Göteborg, Sweden

3. Physik-Institut, Universität Zürich 3 , Winterthurerstrasse 190, CH-8057 Zürich, Switzerland

4. Laboratory for Muon Spin Spectroscopy, Paul Scherrer Institute 4 , Villigen PSI, Switzerland

5. Structure and Mechanics of Advanced Materials, Paul Scherrer Institut 5 , CH-5232 Villigen PSI, Switzerland

6. Deutsches Elektronen-Synchrotron DESY 6 , Notkestraße 85, 22607 Hamburg, Germany

7. Department of Engineering and Applied Sciences, Sophia University 7 , Chiyoda, Tokyo, 102-8554, Japan

Abstract

We present an in situ uniaxial pressure device optimized for small angle x-ray and neutron scattering experiments at low-temperatures and high magnetic fields. A stepper motor generates force, which is transmitted to the sample via a rod with an integrated transducer that continuously monitors the force. The device has been designed to generate forces up to 200 N in both compressive and tensile configurations, and a feedback control allows operating the system in a continuous-pressure mode as the temperature is changed. The uniaxial pressure device can be used for various instruments and multiple cryostats through simple and exchangeable adapters. It is compatible with multiple sample holders, which can be easily changed depending on the sample properties and the desired experiment and allow rapid sample changes.

Funder

JSPS KAKENHI

Swiss National Science Foundation

German Academic Scholarship Foundation

HORIZON EUROPE Marie Sklodowska-Curie Actions

Chalmers X-Ray and Neutron Initiatives

Swedish Research Council

Chalmers Tekniska Högskola, Area of Advance—Material Sciences

Publisher

AIP Publishing

Subject

Instrumentation

Reference41 articles.

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