Transient liquid phase bonding technique for ultrahigh-vacuum compatible bimorph mirrors used in soft x-ray beamlines

Author:

Yuan Debo1ORCID,Liu Zhengkun1ORCID,Xiong Ying1,Zhou Zhiyong2ORCID,Zhang Guobin13ORCID

Affiliation:

1. National Synchrotron Radiation Laboratory, University of Science and Technology of China 1 , Hefei 230026, China

2. Shanghai Institute of Ceramic, Chinese Academy of Sciences 2 , Shanghai 201899, People’s Republic of China

3. Anhui Laboratory of Advanced Photon Science and Technology, University of Science and Technology of China 3 , Hefei 230026, People’s Republic of China

Abstract

Bimorph mirrors place stringent requirements on the welding technology of silicon substrates and piezoelectric ceramics to ensure their ultrahigh-vacuum compatibility. Conventional welding techniques usually require high temperature and pressure, which have a high impact on the welding substrate, while the use of organic adhesives for bonding does not guarantee their stability in ultrahigh vacuum. Here, the transient liquid phase bonding technology based on an Au–In metal system was studied to meet the requirement for ultrahigh-vacuum application. The microstructure, chemical composition, and related mechanical properties of the bonding at different welding conditions were investigated. Meanwhile, the piezo ceramics and the bond were baked at 150 °C to test the stability. The results show that a stable bonding was achieved between centimeter-scaled single crystal silicon and lead zirconate titanate ceramics at 200 °C temperature and 2.5 MPa pressure, and the piezo ceramics and the bond are not damaged by baking to 150 °C for 48 h.

Funder

National Key Research and Development Program of China

National Natural Science Foundation of China

Publisher

AIP Publishing

Subject

Instrumentation

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