Reactions of MoOCl4 with 1-Methylimidazole, 1,4-Diaminobutane, 2-Methylpyridine, 2-Methylpiperidine, Trimethylsilylimidazole and 1-Methylpyrrolidine
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Published:2019-06-20
Issue:3
Volume:35
Page:1094-1102
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ISSN:0970-020X
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Container-title:Oriental Journal of Chemistry
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language:
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Short-container-title:Orient. J. Chem
Author:
Mangla Vikas1, Singh Gursharan2ORCID
Affiliation:
1. Research Scholar Registered with Punjab Technical University, Kapurthala, 144603 - India. 2. Department of Applied Chemistry, Giani Zail Singh Campus College of Engineering and Technology, Dabwali Road, MRSPTU Bathinda,
Abstract
MoOCl4 reacts with 1-methylimidazole, 4-methylpiperidine and trimethylsilylimidazole (equimolar molar amounts) in solvent CH3CN to provide MoO2Cl4(C3H3N2CH3) [1], MoOCl4(C5H9NHCH3)CH3CN [4] and MoO2Cl2(C3H4N2), [7]. MoOCl4 reacts with twice the moles of 1,4-diaminobutane, 2-methylpyridine, 4-methylpiperidine and 1-methylpyrrolidine in solvent CH3CN to provide: MoOCl4(H2NC4H8NH2)2 [2], MoOCl4(C5H4NCH3), [3], MoOCl4(C5H9NHCH3)2, [5], MoOCl4(C5H9NHCH3)2, [6] and MoO2Cl4(C4H8NCH3)2, [8]. Complexes have been studied by techniques: elemental quantitative analysis, FTIR, 1H NMR, Mass (LC-MS).
Publisher
Oriental Scientific Publishing Company
Subject
Drug Discovery,Environmental Chemistry,Biochemistry,General Chemistry
Reference46 articles.
1. Vasisht, S. K.; Singh, G., VII International Symposium on Organosilicon Chemistry., Kyoto, Japan, 1984, 40. 2. Vasisht, S. K.; Singh, G.; Chaudhary, S., Indian Journal of Chemistry., 1985, 24A, 574-577. 3. Vasisht, SK; Singh, G., Z. Anorg. Gen. Chemistry. , 1985, 526, 161-167. 4. Vasisht, S. K.; Singh, G.; Verma, P. K. Monatshefte fur Chemie., 1986, 117, 177-183. 5. Singh, G.; Mangla, V.; Goyal, M.; Singla, K.; Rani, D., American International Journal of Research in Science, Technology, Engineering & Mathematics., 2014, 8(2), 131-136.
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