Investigation of Nonionophoric Coccidiostat Residues in Feed as a Consequence of Carryover-Reference-Cited by-同舟云学术

Investigation of Nonionophoric Coccidiostat Residues in Feed as a Consequence of Carryover

Published:2018-02-23 Issue:3 Volume:81 Page:482-489
ISSN:0362-028X
Container-title:Journal of Food Protection
language:en
Short-container-title:

Author:

Annunziata Loredana¹,Visciano Pierina²,Stramenga Arianna³,Colagrande Maria Novella¹,Campana Guido¹,Scortichini Giampiero³,Migliorati Giacomo¹,Compagnone Dario²

Affiliation:

1. Istituto Zooprofilattico Sperimentale dell'Abruzzo e del Molise “G. Caporale,” Via Campo Boario, 64100 Teramo, Italy;

2. Faculty of Bioscience and Technology for Food, Agriculture, and Environment, University of Teramo, Via R. Balzarini 1, 64100 Teramo, Italy (ORCID: http://orcid.org/0000-0002-3199-5931 [P.V.]); and

3. Istituto Zooprofilattico Sperimentale dell'Umbria e delle Marche, Via G. Salvemini 1, 06126 Perugia, Italy

Abstract

ABSTRACT Residues of nonionophoric coccidiostats at carryover concentrations in feedstuffs collected from feed mills or animal farms in central Italy were detected as part of the official controls carried out from 2011 through 2016. The 118 samples were collected on the production line or during feed distribution and storage to determine the sampling sites at major risk of cross-contamination. For determination of nonionophoric coccidiostats, a fast, easy, and cheap method was developed and validated. Feed samples were extracted with acetonitrile-methanol and directly injected for liquid chromatography with tandem mass spectrometry. A total of 24 samples (20.3%) were positive, but only 5 (4.2%) of these samples exceeded the maximum limit set by European legislation. Most of the positive samples were collected from a batch of feed produced immediately following processing of another batch to which the coccidiostat robenidine had been added.

Publisher

International Association for Food Protection

Subject

Microbiology,Food Science

Link

http://meridian.allenpress.com/jfp/article-pdf/81/3/482/1692548/0362-028x_jfp-17-414.pdf

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