Analysis of Underivatizated Patulin by a GC-MS Technique-Reference-Cited by-同舟云学术

Analysis of Underivatizated Patulin by a GC-MS Technique

Published:1999-02-01 Issue:2 Volume:62 Page:202-205
ISSN:0362-028X
Container-title:Journal of Food Protection
language:en
Short-container-title:

Author:

LLOVERA MONTSERRAT¹,VILADRICH REMEI¹,TORRES MERCÈ²,CANELA RAMON¹³

Affiliation:

1. 1Chemistry Department, Universitat de Lleida, Rovira Roure, 177, 25198-Lleida, Spain

2. 2Department of Food Technology, Universitat de Lleida, Rovira Roure, 177, 25198-Lleida, Spain

3. 3Area de Protecció de Conreus, Centre R+D de Lleida (UdL-IRTA), Rovira Roure, 177, 25198-Lleida, Spain

Abstract

An alternative approach based on the use of gas chromatography-mass spectrometry (GC-MS) is used to confirm the presence of patulin in apple juice. In the gas chromatography (GC) methods previously described, derivatization of patulin was always necessary in order to achieve good chromatographic detection. The use of electronic pressure control (EPC) and on-column injection avoids the need for patulin derivatization and allows a sensitive analysis of patulin. A detection limit of 4 μg/liter in apple juice can be attributed to the method.

Publisher

International Association for Food Protection

Subject

Microbiology,Food Science

Link

http://meridian.allenpress.com/jfp/article-pdf/62/2/202/1665731/0362-028x-62_2_202.pdf

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