A green chemical route for the synthesis of Mn3O4 nanoparticles

Author:

Durmus Zehra1,Kavas Hüseyin2,Baykal Abdulhadi1,Toprak Muhammet3

Affiliation:

1. 1Department of Chemistry, Fatih University, 34500, Istanbul, Turkey

2. 2Department of Physics, Fatih University, 34500, Istanbul, Turkey

3. 3Functional Materials Division, Royal Institute of Technology, SE16440, Stockholm, Sweden

Abstract

AbstractA novel environmental friendly, room temperature route using an ionic liquid 1-n-butyl-3-methylimidazolium hydroxide ([BMIM]OH) for the synthesis of Mn3O4 nanoparticles is presented. The product was characterized using Fourier transform infrared spectroscopy, X-ray powder diffraction, and transmission electron microscopy. Phase purity was confirmed by XRD, and X-ray line profile fitting determined a crystallite size of 42 ± 11 nm. TEM analysis revealed various morphologies. EPR measurements have indicated the existence of long-range interactions, due to the wide range of particle sizes and morphologies observed.

Publisher

Walter de Gruyter GmbH

Subject

Materials Chemistry,General Chemistry

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5. http dx org;Ching;Chem Mater,1997

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