Photochemical Flow Oximation of Alkanes-Reference-Cited by-同舟云学术

Photochemical Flow Oximation of Alkanes

Published:2020-09-21 Issue:19 Volume:31 Page:1907-1912
ISSN:0936-5214
Container-title:Synlett
language:en
Short-container-title:Synlett

Author:

Baxendale Ian R.¹,Griffiths Oliver M.¹²,Ruggeri Michele¹

Affiliation:

1. Department of Chemistry, University of Durham

2. Department of Chemistry, Cambridge University

Abstract

AbstractThe nitrosation of several alkanes using tert-butyl nitrite has been performed in flow showing a remarkable reduction in the reaction time compared with batch processing. Due to the necessity for large excesses of the alkane component a continuous recycling process was devised for the preparation of larger quantities of material.

Publisher

Georg Thieme Verlag KG

Subject

Organic Chemistry

Link

http://www.thieme-connect.de/products/ejournals/pdf/10.1055/s-0040-1707281.pdf

Reference11 articles.

1. Coordination chemistry and metal-involving reactions of amidoximes: Relevance to the chemistry of oximes and oxime ligands

2. Comprehensive Organic Name Reactions and Reagents

3. Continuous generation, in-line quantification and utilization of nitrosyl chloride in photonitrosation reactions

4. Pd-Catalyzed Semmler–Wolff Reactions for the Conversion of Substituted Cyclohexenone Oximes to Primary Anilines

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1. Water-mediated decarboxylative radical nitrosation of β-keto acids with tert-butyl nitrite: access to α-oximino ketones;New Journal of Chemistry;2022

2. Continuous flow technology-a tool for safer oxidation chemistry;Reaction Chemistry & Engineering;2022

3. Cluster Preface: Integrated Synthesis Using Continuous-Flow Technologies;Synlett;2020-11-17