Continuous generation, in-line quantification and utilization of nitrosyl chloride in photonitrosation reactions-Reference-Cited by-同舟云学术

Continuous generation, in-line quantification and utilization of nitrosyl chloride in photonitrosation reactions

Published:2019 Issue:4 Volume:4 Page:738-746
ISSN:2058-9883
Container-title:Reaction Chemistry & Engineering
language:en
Short-container-title:React. Chem. Eng.

Author:

Lebl René¹²³⁴⁵,Cantillo David¹²³⁴⁵,Kappe C. Oliver¹²³⁴⁵^ORCID

Affiliation:

1. Center for Continuous Flow Synthesis and Processing (CCFLOW)

2. Research Center Pharmaceutical Engineering GmbH (RCPE)

3. 8010 Graz

4. Austria

5. Institute of Chemistry

Abstract

The reagent is prepared from stable, inexpensive and readily available starting materials. In-line UV/vis monitoring enables determination of the reagent's concentration after a continuous extraction and liquid–liquid separation sequence.

Funder

Österreichische Forschungsförderungsgesellschaft

Publisher

Royal Society of Chemistry (RSC)

Subject

Fluid Flow and Transfer Processes,Process Chemistry and Technology,Chemical Engineering (miscellaneous),Chemistry (miscellaneous),Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2019/RE/C8RE00323H

Reference60 articles.

1. Nitrosyl Chloride.

2. D. Lyn , H.Williams and V.Sikervar , in Encyclopedia of Reagents for Organic Synthesis , John Wiley & Sons, Ltd , Chichester, UK , 2014 , vol. 1 , pp. 1–3

3. XXXII.—On aqua regia and the nitrosyl chlorides

4. XIX.—Isomeric nitroso-terpenes

5. XXXV.—Action of nitrosyl chloride on unsaturated compounds

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