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SABRE enhancement with oscillating pulse sequences

Published:2022 Issue:27 Volume:24 Page:16462-16470
ISSN:1463-9076
Container-title:Physical Chemistry Chemical Physics
language:en
Short-container-title:Phys. Chem. Chem. Phys.

Author:

Li Xiaoqing¹^ORCID,Lindale Jacob R.²^ORCID,Eriksson Shannon L.²³,Warren Warren S.¹²⁴

Affiliation:

1. Department of Physics, Duke University Durham, NC 27708, USA

2. Department of Chemistry, Duke University Durham, NC 27708, USA

3. School of Medicine, Duke University Durham, NC 27708, USA

4. Department of Biomedical Engineering, and Radiology, Duke University, Durham, NC (27708), USA

Abstract

Oscillating pulse SABRE (Signal Amplification by Reversible Exchange) that uses magnetic fields far away from the resonance condition of continuous excitation can triple the polarization. The oscillating pulse, in effect, adjusts the J-couplings between hydrides and target nuclei.

Funder

National Science Foundation

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Link

http://pubs.rsc.org/en/content/articlepdf/2022/CP/D2CP00899H

Reference32 articles.

1. Increase in signal-to-noise ratio of > 10,000 times in liquid-state NMR

2. Spin-exchange optical pumping of noble-gas nuclei

3. Para hydrogen induced polarization in hydrogenation reactions

4. Parahydrogen and synthesis allow dramatically enhanced nuclear alignment

5. Reversible Interactions with para-Hydrogen Enhance NMR Sensitivity by Polarization Transfer

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1. Development of a fully automated workstation for conducting routine SABRE hyperpolarization;Scientific Reports;2024-09-09

2. NMRduino: A modular, open-source, low-field magnetic resonance platform;Journal of Magnetic Resonance;2024-05

3. Multi-axis fields boost SABRE hyperpolarization;Proceedings of the National Academy of Sciences;2024-03-27

4. Hyperpolarisation techniques;Nuclear Magnetic Resonance;2023-11-29

5. Parahydrogen-based NMR signal amplification by reversible exchange (SABRE): Recent advances and applications;Mendeleev Communications;2023-09

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