Synthesis, structure and reactivity of η4(5e)-butadienyl substituted molybdenum complexes
Author:
Publisher
Royal Society of Chemistry (RSC)
Subject
General Chemistry
Link
http://pubs.rsc.org/en/content/articlepdf/1996/DT/DT9960004517
Reference36 articles.
1. Reaction of the η2(4e)-donor alkyne complexes [Mo{η2(4e)-R1C2R2}{P(OMe)3}2(η-C5H5)](R1= R2= Ph or Me; R1= Me, R2= Ph) with the Grignard reagents MgR3(X)(R3= Me, Et, CH2Ph, CH2CHCH2or CHCH2) and CH2(MgI)2
2. Reaction of cationic cyclobutadineruthenium complexes with hydride anion donors; evidence for the formation of η4(5e) butadienyl species and fragmentation of the cyclobutadiene ring: crystal structure of [RuC(Ph)–η3-{C(Ph)·CH(Ph)·CH(Ph)}-(η-C5H5)] and [Ru2(µ-CO){µ-(Z)-C(Ph)CH(Ph)}(CO)2(η4-C4Ph4)(η-C5H5)]
3. Reactions of coordinated ligands. Part 47. Synthesis, structure, and reactivity of [.eta.4(5e)-butadienyl]ruthenium complexes: crystal structures of CpRu:C(Ph)-.eta.3-[C(Ph)C(Ph)CH(Ph)], CpRuC(Ph):C(Ph)-.eta.2-[C(Ph):CH(Ph)]P(OMe)3, and CpRu2[.mu.-(Z)-C(Ph):CH(Ph)](CO)2(.eta.4-C4Ph4)
4. Protonation of molybdenum(II) and tungsten(II) bis(alkyne) complexes: formation of .eta.4-C4R4H ligands
5. The mechanistic role of η2-vinyl complexes in metal-promoted alkyne oligomerisations. The crystal and molecular structures of [W{η5-C(CF3)C(CF3)C(CO2Me )C(CO2Me)C(CF3)C(CF3)SPri}(η5-C5H5)], [WF {η5-C(CF2)C(CF3)C( CO2Me)C( CO2Me)C(CF3)C(CF3)SPri}(η5-C5H5)], and [W{η4-C(CF3)C(CF3)C(Me)C(Me)SPri}(η2-CF3CCCF3)(η5-C5H5)]
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