Synthesis and modification of monodisperse silica microspheres for UPLC separation of C60 and C70-Reference-Cited by-同舟云学术

Synthesis and modification of monodisperse silica microspheres for UPLC separation of C60 and C70

Published:2016 Issue:4 Volume:8 Page:919-924
ISSN:1759-9660
Container-title:Analytical Methods
language:en
Short-container-title:Anal. Methods

Author:

Yu Bing¹²³⁴⁵,Cong Hailin¹²³⁴⁵,Xue Lei¹²³⁴⁵,Tian Chao¹²³⁴⁵,Xu Xiaodan¹²³⁴⁵,Peng Qiaohong¹²³⁴⁵,Yang Shujing¹²³⁴⁵

Affiliation:

1. Laboratory for New Fiber Materials and Modern Textile

2. Growing Base for State Key Laboratory

3. College of Chemical Engineering

4. Qingdao University

5. China

Abstract

Using a modified Stöber method, monodisperse silica microspheres with average diameters from 1 μm to 2 μm are synthesized as UPLC column fillers. With a column as short as 50 mm, the 1.5 μm C₁₈-modified silica stationary phase can separate C₆₀ and C₇₀ in 7 minutes with ultra high efficiency.

Publisher

Royal Society of Chemistry (RSC)

Subject

General Engineering,General Chemical Engineering,Analytical Chemistry

Link

http://pubs.rsc.org/en/content/articlepdf/2016/AY/C5AY02655E

Reference28 articles.

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