Liquid-phase synthesis of highly oxophilic zerovalent niobium and tantalum nanoparticles-Reference-Cited by-同舟云学术

Liquid-phase synthesis of highly oxophilic zerovalent niobium and tantalum nanoparticles

Published:2021 Issue:30 Volume:57 Page:3648-3651
ISSN:1359-7345
Container-title:Chemical Communications
language:en
Short-container-title:Chem. Commun.

Author:

Egeberg Alexander¹²³⁴⁵,Faden Lara-Pauline¹²³⁴⁵,Zimina Anna⁶²⁷⁸⁵,Grunwaldt Jan-Dierk⁶²⁷⁸⁵^ORCID,Gerthsen Dagmar⁹²¹⁰⁴⁵,Feldmann Claus¹²³⁴⁵^ORCID

Affiliation:

1. Institute for Inorganic Chemistry

2. Karlsruhe Institute of Technology (KIT)

3. Engesserstrasse 15

4. Karlsruhe 76131

5. Germany

6. Institute of Catalysis Research and Technology

7. Hermann-von-Helmholtz-Platz 1

8. Eggenstein-Leopoldshafen 76344

9. Laboratory for Electron Microscpy

10. Engesserstrasse 7

Abstract

Zerovalent Nb(0) and Ta(0) nanoparticles are prepared via a one-pot, liquid-phase synthesis for the first time. This is a challenge due to the basic and highly oxophilic character of both metals.

Funder

Deutsche Forschungsgemeinschaft

Publisher

Royal Society of Chemistry (RSC)

Subject

Materials Chemistry,Metals and Alloys,Surfaces, Coatings and Films,General Chemistry,Ceramics and Composites,Electronic, Optical and Magnetic Materials,Catalysis

Link

http://pubs.rsc.org/en/content/articlepdf/2021/CC/D1CC00681A

Reference23 articles.

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2. Y. Freeman , Tantalum and Niobium-Based Capacitors , Springer , Berlin , 2018

3. Direct synthesis of Nb–Al intermetallic nanoparticles by sodiothermic homogeneous reduction in molten salts

4. Preparation of niobium nanoparticles by sodiothermic reduction of Nb2O5 in molten salts

5. Tantalum and niobium powder preparation from their oxides by calciothermic reduction in the molten CaCl2

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