Step-by-step from amorphous phosphate to nano-structured calcium hydroxyapatite: monitoring by solid-state 1H and 31P NMR and spin dynamics

Author:

Klimavicius Vytautas1,Maršalka Arūnas1,Kizalaite Agne2,Zarkov Aleksej2ORCID,Kareiva Aivaras2,Aidas Kęstutis1ORCID,Hirschinger Jérôme3ORCID,Balevicius Vytautas1ORCID

Affiliation:

1. Institute of Chemical Physics, Vilnius University, LT-10257 Vilnius, Lithuania

2. Institute of Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania

3. Institut de Chimie, Université de Strasbourg, UMR 7177 CNRS, Strasbourg, France

Abstract

Structural and dynamical evolution in a series of samples including amorphous phosphate, composite, and nano-structured calcium hydroxyapatite is probed by NMR cross-polarization kinetics.

Funder

European Social Fund

Publisher

Royal Society of Chemistry (RSC)

Subject

Physical and Theoretical Chemistry,General Physics and Astronomy

Reference53 articles.

1. Calcium phosphates in biomedical applications: materials for the future?

2. P. W.Brown and B.Constantz , Hydroxyapatite and Related Materials , CRC Press , 1994

3. R. Z.Le Geros and J. P.Le Geros , in Bioceramics and Their Clinical Applications , ed. T. Kokubo , Woodhead Publishing , Cambridge , 2008

4. Influence of Temperature on Calcium Hydroxyapatite Nanopowders

5. Dissolution–Precipitation Synthesis and Characterization of Zinc Whitlockite with Variable Metal Content

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