Quick temperature-sweep pure-shift NMR: the case of solvent effects in atorvastatin
Author:
Affiliation:
1. Centre of New Technologies
2. University of Warsaw
3. 02-097 Warsaw
4. Poland
5. Department of Mathematical Methods in Physics
Abstract
Quick and sensitive serial pseudo-2D pure-shift NMR experiments provide novel insight into the temperature-dependent solvent distribution.
Funder
European Molecular Biology Organization
Fundacja na rzecz Nauki Polskiej
Publisher
Royal Society of Chemistry (RSC)
Subject
Physical and Theoretical Chemistry,General Physics and Astronomy
Link
http://pubs.rsc.org/en/content/articlepdf/2019/CP/C9CP03921J
Reference28 articles.
1. C. Reichardt and T.Welton , Solvents and Solvent Effects in Organic Chemistry , Wiley-VCH , Weinheim , 4th edn, 2011
2. Pure shift NMR
3. Ultrahigh-Resolution NMR Spectroscopy
4. Measuring couplings in crowded NMR spectra: pure shift NMR with multiplet analysis
5. Enabling Fast Pseudo-2D NMR Spectral Acquisition for Broadband Homonuclear Decoupling: The EXACT NMR Approach
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