Supporting the assignment of NMR spectra with variable‐temperature experiments

Author:

Nawrocka Ewa K.1,Jadwiszczak Michał1,Leszczyński Piotr J.1,Kazimierczuk Krzysztof1ORCID

Affiliation:

1. Centre of New Technologies University of Warsaw Warsaw Poland

Abstract

AbstractNuclear magnetic resonance (NMR) spectroscopy is one of the most powerful tools in analytical chemistry. An important step in the analysis of NMR data is the assignment of resonance frequencies to the corresponding atoms in the molecule being investigated. The traditional approach considers the spectrum's characteristic parameters: chemical shift values, internuclear couplings, and peak intensities. In this paper, we show how to support the process of assigning a series of spectra of similar organic compounds by using temperature coefficients, that is, the rates of change in chemical shift values associated with given changes in temperature.

Funder

Narodowe Centrum Nauki

Publisher

Wiley

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