Measurement and alleviation of subsurface damage in a thick-crystal neutron interferometer
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Published:2019-10-07
Issue:6
Volume:75
Page:833-841
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ISSN:2053-2733
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Container-title:Acta Crystallographica Section A Foundations and Advances
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language:
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Short-container-title:Acta Cryst Sect A
Author:
Heacock Benjamin,Haun Robert,Hirota Katsuya,Hosobata Takuya,Huber Michael G.,Jamer Michelle E.,Kitaguchi Masaaki,Pushin Dmitry A.,Shimizu Hirohiko,Taminiau Ivar,Yamagata Yutaka,Yamamoto Tomoki,Young Albert R.
Abstract
The construction is described of a monolithic thick-crystal perfect silicon neutron interferometer using an ultra-high-precision grinding technique and a combination of annealing and chemical etching that differs from the construction of prior neutron interferometers. The interferometer is the second to have been annealed after machining and the first to be annealed prior to chemical etching. Monitoring the interference signal at each post-fabrication step provides a measurement of subsurface damage and its alleviation. In this case, the strain caused by subsurface damage manifests itself as a spatially varying angular misalignment between the two relevant volumes of the crystal and is reduced from ∼10−5 rad to ∼10−9 rad by way of annealing and chemical etching.
Funder
U.S. Department of Energy
National Science Foundation
National Institute of Standards and Technology
Canada Excellence Research Chairs, Government of Canada
Canada First Research Excellence Fund
Natural Sciences and Engineering Research Council of Canada
Publisher
International Union of Crystallography (IUCr)
Subject
Inorganic Chemistry,Physical and Theoretical Chemistry,Condensed Matter Physics,General Materials Science,Biochemistry,Structural Biology
Cited by
2 articles.
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