Mosher ester analysis for the determination of absolute configuration of stereogenic (chiral) carbinol carbons
Author:
Publisher
Springer Science and Business Media LLC
Subject
General Biochemistry, Genetics and Molecular Biology
Link
http://www.nature.com/articles/nprot.2007.354.pdf
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3. Dale, J.A. & Mosher, H.S. Nuclear magnetic resonance enantiomer reagents. Configurational correlations via nuclear magnetic resonance chemical shifts of diastereomeric mandelate, O-methylmandelate, and α-methoxy-α-trifluoromethylphenylacetate (MTPA) esters. J. Am. Chem. Soc. 95, 512–519 (1973).
4. Hoye, T.R. & Renner, M.K. MTPA (Mosher) amides of cyclic secondary amines: conformational aspects and a useful method for assignment of amine configuration. J. Org. Chem. 61, 2056–2064 (1996).
5. Dale, J.A., Dull, D.L. & Mosher, H.S. α-Methoxy-α-trifluoromethylphenylacetic acid, a versatile reagent for the determination of enantiomeric composition of alcohols and amines. J. Org. Chem. 34, 2543–2549 (1969).
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