Reactive trans-dimetallated alkenes from alkynes
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Publisher
Springer Science and Business Media LLC
Link
https://www.nature.com/articles/s44160-022-00190-6.pdf
Reference4 articles.
1. Juhász, K., Magyar, Á. & Hell, Z. Transition-metal-catalyzed cross-coupling reactions of Grignard reagents. Synthesis 53, 983–1002 (2021). A review article that presents the utility of Grignard reagents in modern organic synthesis.
2. Levin, G., Jagur-Grodzinski, J. & Szwarc, M. Chemistry of radical anions and dianions of diphenylacetylene. J. Am. Chem. Soc. 92, 2268–2275 (1970). This paper reports the instability of 1,2-dimetallated species.
3. Dange, D. et al. Acyclic 1,2-dimagnesioethanes/-ethene derived from magnesium(i) compounds: multipurpose reagents for organometallic synthesis. Chem. Sci. 10, 3208–3216 (2019). This paper reports an example of the synthesis of 1,2-dimetallated species starting from a highly elaborate inorganic precursor.
4. Fukazawa, M., Takahashi, F., Nogi, K., Sasamori, T. & Yorimitsu, H. Reductive difunctionalization of aryl alkenes with sodium metal and reduction-resistant alkoxy-substituted electrophiles. Org. Lett. 22, 2303–2307 (2020). This paper reports the use of trialkoxyboranes as reduction-resistant electrophiles.
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