Determining the Crystal Structures of Peptide Analogs of Boronic Acid in the Absence of Single Crystals: Intricate Motifs of Ixazomib Citrate Revealed by XRPD Guided by ss-NMR-Reference-Cited by-同舟云学术

Determining the Crystal Structures of Peptide Analogs of Boronic Acid in the Absence of Single Crystals: Intricate Motifs of Ixazomib Citrate Revealed by XRPD Guided by ss-NMR

Published:2018-04-30 Issue:6 Volume:18 Page:3616-3625
ISSN:1528-7483
Container-title:Crystal Growth & Design
language:en
Short-container-title:Crystal Growth & Design

Author:

Hušák Michal¹,Jegorov Alexandr²,Rohlíček Jan³,Fitch Andrew⁴,Czernek Jiří⁵,Kobera Libor⁵^ORCID,Brus Jiří⁵^ORCID

Affiliation:

1. Department of Solid State Chemistry, University of Chemistry and Technology, Technicka 5, 166 28 Prague 6, Czech Republic

2. Teva Pharmaceuticals CR, s.r.o., Branisovska 31, 370 05 Ceske Budejovice, Czech Republic

3. Department of Structural Analysis, Institute of Physics of the Czech Academy of Sciences, Na Slovance 2, Praha 8, 182 21, Czech Republic

4. ESRF, The European Synchrotron, CS40220, F-38043 Grenoble Cedex 9, France

5. Department of NMR Spectroscopy, Institute of Macromolecular Chemistry CAS, Heyrovsky sq. 2, 162 06 Prague 6, Czech Republic

Funder

Ministerstvo ?kolstv?, Ml?de?e a Telov?chovy

Grantov? Agentura Cesk? Republiky

Publisher

American Chemical Society (ACS)

Subject

Condensed Matter Physics,General Materials Science,General Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/acs.cgd.8b00402

Reference51 articles.

1. Decitabine for the treatment of acute myeloid leukemia

2. DNA Methyltransferase-1 Inhibitors as Epigenetic Therapy for Cancer

3. Chemical Decomposition of 5-Aza-2′-deoxycytidine (Decitabine): Kinetic Analyses and Identification of Products by NMR, HPLC, and Mass Spectrometry

4. Spirocyclic character of ixazomib citrate revealed by comprehensive XRD, NMR and DFT study

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