1. Department of Materials, Loughborough University, Loughborough, Leicestershire LE11 3TU, U.K.
2. School of Metallurgy and Materials, College of Engineering and Physical Sciences, University of Birmingham, Edgbaston, Birmingham B15 2TT, U.K.
3. Institut Max von Laue-Paul Langevin (ILL), F-38042 Grenoble Cedex 9, France