1. Innovative Technology Centre, Department of Chemistry, University of Cambridge, Lensfield Road, Cambridge CB2 1EW, U.K., Mettler-Toledo AutoChem, 7075 Samuel Morse Drive, Columbia, Maryland 21046, U.S.A., Mettler-Toledo AutoChem UK, 64 Boston Road, Beaumont Leys, Leicester LE4 1AW, UK