Optimization of Organolithium Reactions-Reference-Cited by-同舟云学术

Optimization of Organolithium Reactions

Published:2008-12-10 Issue:2 Volume:13 Page:144-151
ISSN:1083-6160
Container-title:Organic Process Research & Development
language:en
Short-container-title:Org. Process Res. Dev.

Author:

Rathman Terry ‘Li’¹,Bailey William F.¹

Affiliation:

1. t-Links Consulting, 100-29 Willow Run, Gastonia, North Carolina 28056, U.S.A., and Department of Chemistry, The University of Connecticut, Storrs, Connecticut 06269 U.S.A.

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Physical and Theoretical Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/op800246z

Reference55 articles.

1. Morrison, R. C. and Rathman, T. L.Preparation of organometallic and organobimetallic compounds. (Lithium Corp. of America). U.S. Pat. 4,976,886, 1990.

2. The use of 2 equiv ofn-BuLi to prepare the MeLi−LiI complex was not explored, nor was the use of methyl bromide instead of methyl iodide investigated.

3. In the 1970s, FMC Lithium metalated 1,3-dimethoxybenzene in hydrocarbon withn-BuLi at ambient temperature and at reflux. The resulting 2,6-dimethoxy-phenyllithium was only sparingly soluble in the medium.

4. The synthesis of 1,2,3-trisubstituted benzenes. Further comments on benzynes derived from aryl oxazolines

5. aLipton, M. F.; Mauragis, M. A.; Veley, M. F.; Bundy, G. L.; Bannitt, L. S.; Doberwolski, P. J.; Palmer, J. R.; Schwartz, T. M.; Zimmerman, D. C.From Bench to Pilot Plant, Process Research in the Pharmaceutical Industry; ACS Symposium Series; 2001; p101.

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