1. Graduate School of Life and Environmental Sciences, University of Tsukuba, 1-1-1, Tennoudai, Tsukuba, Ibaraki, 305-8572, Japan, and Laboratoire Environnement et Minéralurgie, Nancy-University, CNRS, 15 avenue du Charmois, B.P. 40, 54501 Vandoeuvre-les-Nancy cedex, France