1. Contribution from the School of Chemistry, University of Exeter, Stocker Road, Exeter EX4 4QD, UK, Institut Lavoisier, UMR CNRS 8637, Université de Versailles Saint Quentin-en-Yvelines, 45 Avenue des Etats-Unis, 78035 Versailles Cedex, France, ISIS Facility, Rutherford Appleton Laboratory, Chilton, Oxon OX11 0QX, UK, Institut Laue Langevin, F-38042, Grenoble Cedex, France, and Inorganic Chemistry Laboratory, South Parks Road, Oxford OX1 3QR, UK