Reactivity toward CO of Eight-Membered Palladacycles Derived from the Insertion of Alkenes into the Pd–C Bond of Cyclopalladated Primary Arylalkylamines of Pharmaceutical Interest. Synthesis of Tetrahydrobenzazocinones, Ortho-Functionalized Phenethylamines, Ureas, and an Isocyanate
Author:
Affiliation:
1. Grupo de Química Organometálica, Departamento de Química Inorgánica, Facultad de Química, Universidad de Murcia, E-30071 Murcia, Spain
2. SAI, Universidad de Murcia, E-30071 Murcia, Spain
Publisher
American Chemical Society (ACS)
Subject
Inorganic Chemistry,Organic Chemistry,Physical and Theoretical Chemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/om300593x
Reference119 articles.
1. Eight-Membered Palladacycles Derived from the Insertion of Olefins into the Pd−C Bond of Ortho-Palladated Pharmaceuticals Phenethylamine and Phentermine. Synthesis of Stable Heck-Type Intermediates Containing Accessible β-Hydrogens and Its Use in the Synthesis of 2-Styrylphenethylamines, Tetrahydroisoquinolines, and Eight-Membered Cyclic Amidines
2. Insertion of benzyne into the Pd–C bond. Synthesis of unnatural amino acid derivatives by sequential insertion of benzyne and CO: 2,2′-functionalized biaryls containing alkylamino and carboxymethyl substituents. Isolation of stable carbopalladated-benzyne intermediates
3. Sequential Insertion of Alkynes and CO or Isocyanides into the Pd–C Bond of Cyclopalladated Phenylacetamides. Synthesis of Eight-Membered Palladacycles, Benzo[d]azocine-2,4(1H,3H)-diones, and Highly Functionalized Acrylonitrile and Acrylamide Derivatives
4. Monoinsertion of but-2-ynedioic acid dimethyl ester into palladium–carbon σ bonds of cyclopalladated compounds derived from biphenyl-2-ylamine: X-ray molecular structure of biphenyl-2-yl-(2,4,6-trimethoxy-benzylidene)-amine
5. A comparative study of the reactivity of the σ(Pd–Csp2, ferrocene) and σ(Pd–Csp2, biphenyl) bonds in cyclopalladated complexes derived from [Fe(η5-C5H5)(η5-C5H4CHNC6H4C6H5-2)]
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