A Detailed Study of Sulfonate Ester Formation and Solvolysis Reaction Rates and Application toward Establishing Sulfonate Ester Control in Pharmaceutical Manufacturing Processes-Reference-Cited by-同舟云学术

A Detailed Study of Sulfonate Ester Formation and Solvolysis Reaction Rates and Application toward Establishing Sulfonate Ester Control in Pharmaceutical Manufacturing Processes

Published:2010-03-10 Issue:4 Volume:14 Page:999-1007
ISSN:1083-6160
Container-title:Organic Process Research & Development
language:en
Short-container-title:Org. Process Res. Dev.

Author:

Teasdale Andrew¹,Delaney Edward J.¹,Eyley Stephen C.¹,Jacq Karine¹,Taylor-Worth Karen¹,Lipczynski Andrew¹,Hoffmann Wilfried¹,Reif Van¹,Elder David P.¹,Facchine Kevin L.¹,Golec Simon¹,Schulte Oestrich Rolf¹,Sandra Pat¹,David Frank¹

Affiliation:

1. AstraZeneca, R&D Charnwood, Bakewell Road, Loughborough, Leicestershire LE11 5RH, United Kingdom; Reaction Science Consulting LLC, 11 Deer Park Drive/Suite 202, Monmouth Junction, New Jersey 08852, U.S.A.; Research Institute for Chromatography, Pres. Kennedypark 26, B-8500, Kortrijk, Belgium; Pfizer Global Research and Development, Analytical R&D, Ramsgate Road, Sandwich, Kent CT13 9NJ, United Kingdom; Schering-Plough, 556 Morris Avenue, Summit, New Jersey 07901-1330, U.S.A.; GlaxoSmithKline, Park Road,...

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Physical and Theoretical Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/op900301n

Reference11 articles.

1. Mechanism and Processing Parameters Affecting the Formation of Methyl Methanesulfonate from Methanol and Methanesulfonic Acid: An Illustrative Example for Sulfonate Ester Impurity Formation

2. Development and validation of an automated static headspace gas chromatography–mass spectrometry (SHS-GC–MS) method for monitoring the formation of ethyl methane sulfonate from ethanol and methane sulfonic acid

3. Control and analysis of alkyl esters of alkyl and aryl sulfonic acids in novel active pharmaceutical ingredients (APIs)

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