First Unambiguous Characterization of a Novel RO-BH2 Intermediate by 1H{11B} and 1H{13C,11B} NMR Spectroscopy. Proof of Boron−Carbonyl Interaction through Innovative Use of NMR Techniques
Author:
Affiliation:
1. Department of Chemistry, University of Wisconsin−Milwaukee, 3210 N. Cramer Street, Milwaukee, Wisconsin 53211
Publisher
American Chemical Society (ACS)
Subject
Inorganic Chemistry,Organic Chemistry,Physical and Theoretical Chemistry
Link
https://pubs.acs.org/doi/pdf/10.1021/om800137q
Reference12 articles.
1. Asymmetric boron-catalyzed reactions
2. Boron Reagents in Process Chemistry: Excellent Tools for Selective Reductions
3. Boron-11 nuclear magnetic resonance study of the reactions of 2-functionalized pyridines with borane–tetrahydrofuran and –dimethyl sulphide. Formation of borinic estes and N → B bond energy differences in five- and six-membered ring borates
4. Exceptionally slow reduction of phenylmalonic acid by borane-tetrahydrofuran via cyclic (phenylmalonoxy)borane
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