Diazo-Transfer Reagent 2-Azido-4,6-dimethoxy-1,3,5-triazine Displays Highly Exothermic Decomposition Comparable to Tosyl Azide-Reference-Cited by-同舟云学术

Diazo-Transfer Reagent 2-Azido-4,6-dimethoxy-1,3,5-triazine Displays Highly Exothermic Decomposition Comparable to Tosyl Azide

Published:2019-04-05 Issue:9 Volume:84 Page:5893-5898
ISSN:0022-3263
Container-title:The Journal of Organic Chemistry
language:en
Short-container-title:J. Org. Chem.

Author:

Green Sebastian P.¹²,Payne Andrew D.³,Wheelhouse Katherine M.⁴,Hallett Jason P.²^ORCID,Miller Philip W.¹^ORCID,Bull James A.¹^ORCID

Affiliation:

1. Department of Chemistry, Molecular Sciences Research Hub, Imperial College London, White City Campus, 80 Wood Lane, London W12 0BZ, U.K.

2. Department of Chemical Engineering, Imperial College London, South Kensington Campus, Exhibition Road, London SW7 2AZ, U.K.

3. Process Safety, Pilot Plant Operations, GlaxoSmithKline, GSK Medicines Research Centre, Gunnels Wood Road, Stevenage, Hertfordshire SG1 2NY, U.K.

4. API Chemistry, Product Development & Supply, GlaxoSmithKline, GSK Medicines Research Centre, Gunnels Wood Road, Stevenage, Hertfordshire SG1 2NY, U.K.

Funder

Engineering and Physical Sciences Research Council

Royal Society

GlaxoSmithKline

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/acs.joc.9b00269

Reference31 articles.

1. New Syntheses of Diazo Compounds

2. A Safer Diazotransfer Reagent

3. Identification of a safe diazotransfer reagent

4. Diazotransfer Reagents1

5. New Methods of Preparative Organic Chemistry. Transfer of Diazo Groups

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