Selective Crystallization of an Allylic 7α-Bromide: A Facile Synthesis of (1α,3β)-3-Hydroxycholeste-5,7-diene-1,25-diol Diacetate-Reference-Cited by-同舟云学术

Selective Crystallization of an Allylic 7α-Bromide: A Facile Synthesis of (1α,3β)-3-Hydroxycholeste-5,7-diene-1,25-diol Diacetate

Published:2005-03-23 Issue:3 Volume:9 Page:306-310
ISSN:1083-6160
Container-title:Organic Process Research & Development
language:en
Short-container-title:Org. Process Res. Dev.

Author:

Van Arnum Susan D.¹,Carpenter Barry K.¹,Moffet Harold¹,Parrish David R.¹,MacIntrye Archibald¹,Cleary Thomas P.¹,Fritch Paul¹

Affiliation:

1. Pharmaceutical Process Development, Hoffmann-La Roche, 340 Kingsland Avenue, Nutley, New Jersey 07110, U.S.A., and Department of Chemistry and Chemical Biology, Cornell University, Ithaca, New York 14853, U.S.A.

Publisher

American Chemical Society (ACS)

Subject

Organic Chemistry,Physical and Theoretical Chemistry

Link

https://pubs.acs.org/doi/pdf/10.1021/op050009r

Reference14 articles.

1. Process Control Limits from a Laboratory Study on the Ni(0)-Mediated Coupling of Ethyl Acrylate with a C-22 Steroidal Iodide: A Case Study on the Role of Experimental Design in Highly Developed Processes

2. An Improved Synthesis of the Selective Matrix Metalloproteinase Inhibitor, Ro 28-2653

3. The Preparation of (1α,3β)-3-Hydroxycholestane-4,6-diene- 1,25-diol Diacetate from a 5,7-Diene Precursor: A New Method for the Synthesis of Heteroannular Dienes

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