Morphological Analyses of W/Cu Functional Graded Materials Obtained by Conventional and Spark Plasma Sintering

Author:

Nicolicescu Claudiu1,Nicoară Victor Horia1,Pascu Cristina Ileana1ORCID,Gheorghe Ștefan1,Burada Cristian Oliviu1,Marinca Traian Florin2ORCID,Popa Florin2ORCID

Affiliation:

1. Faculty of Mechanics, University of Craiova, 200512 Craiova, Romania

2. Faculty of Materials Engineering and Environment, Technical University of Cluj-Napoca, 400641 Cluj-Napoca, Romania

Abstract

The paper presents the analysis of two compaction methods for obtaining W/Cu Functional Graded Materials (FGMs) consisting of three layers with the following compositions (% weight): first layer 80 W/20 Cu, second layer 75 W/25 Cu, and third layer 65 W/35 Cu. Each layer composition was obtained using powders obtained through mechanical milling. The two compaction methods were Spark Plasma Sintering (SPS) and Conventional Sintering (CS). The samples obtained after the SPS and CS were investigated from morphological (scanning electron microscopy-SEM) and compositional (energy dispersive X-ray spectroscopy-EDX) points of views. Additionally, the porosities and the densities of each layer in both cases were studied. It was found that the densities of the sample’s layers obtained through SPS are superior to those obtained through CS. The research emphasizes that, from a morphological point of view, the SPS process is recommended for W/Cu-FGMs, having raw materials as fine-graded powders against the CS process.

Publisher

MDPI AG

Subject

General Materials Science

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