Magnetic-Dielectric Cantilevers for Atomic Force Microscopy

Author:

Sanchez-Seguame Gala1,Avalos-Sanchez Hugo1,Eduardo Lugo Jesus123,Murillo-Bracamontes Eduardo Antonio4,Palomino-Ovando Martha Alicia1,Hernández-Cristobal Orlando5,Gervacio-Arciniega José Juan6ORCID,Toledo-Solano Miller6ORCID

Affiliation:

1. Facultad de Ciencias Físico-Matemáticas, Benemérita Universidad Autónoma de Puebla, Av. San Claudio y Av. 18 sur, Col. San Manuel Ciudad Universitaria, Puebla Pue 72570, Mexico

2. Faubert Lab, School of Optometry, University of Montreal, Montreal, QC H3T1P1, Canada

3. Sage-Sentinel Smart Solutions, 1919-1 Tancha, Onna-son, Kunigami-gun, Okinawa 904-0495, Japan

4. Centro de Nanociencias y Nanotecnología, Universidad Nacional Autónoma de México, Ensenada 22800, Mexico

5. Escuela Nacional de Estudios Superiores, Universidad Nacional Autónoma de México, Antigua Carretera a Pátzcuaro 8701, Colonia San José de la Huerta, Morelia 58089, Mexico

6. Consejo Nacional de Humanidades, Ciencias y Tecnologías-Facultad de Ciencias Físico-Matemáticas, Benemérita Universidad Autónoma de Puebla, Av. San Claudio y Av. 18 sur, Col. San Manuel Ciudad Universitaria, Puebla Pue 72570, Mexico

Abstract

Atomic force microscopy (AFM) is a technique that relies on detecting forces at the nanonewton scale. It involves using a cantilever with a tiny tip at one end. This tip interacts with the short- and long-range forces of material surfaces. These cantilevers are typically manufactured with Si or Si3N4 and synthesized using a lithography technique, which implies a high cost. On the other hand, through simple chemical methods, it is possible to synthesize a magneto-dielectric composite made up of artificial SiO2 opals infiltrated with superparamagnetic nanoparticles of Fe3O4. From these materials, it is possible to obtain tipless cantilevers that can be used in AFM analysis. Tipless cantilevers are an alternative tool in nanoscale exploration, offering a versatile approach to surface analysis. Unlike traditional AFM probes, tipless versions eliminate the challenges associated with tip wear, ensuring prolonged stability during measurements. This makes tipless AFM particularly valuable for imaging delicate or soft samples, as it prevents sample damage and provides precise measurements of topography and mechanical and electromechanical properties. This study presents the results of the characterization of known surfaces using magneto-dielectric cantilevers and commercial cantilevers based on Si. The characterization will be carried out through contact and non-contact topography measurements.

Funder

CONAHCYT

Publisher

MDPI AG

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