A waste hemp‐based biomass carbon aerogel with high fire‐resistance

Author:

Liu Jiangtao12ORCID,Yang Ke3,Yang Yaru4,Zhang Mingshuo1,Shi Yiran1,Xue Baoxia12,Niu Mei12,Zhang Li5

Affiliation:

1. College of Textile Engineering Taiyuan University of Technology Taiyuan China

2. Shanxi‐Zheda Institute of Advanced Materials and Chemical Engineering Taiyuan China

3. CSIC Electrical Machinery Science Technology Co., Ltd Taiyuan China

4. College of Materials and Textile Engineering Jiaxing University Jiaxing China

5. Third Hospital of Shanxi Medical University, Shanxi Bethune Hospital, Shanxi Academy of Medical Sciences, Tongji Shanxi Hospital Taiyuan China

Abstract

AbstractTo enhance the efficient utilization of waste hemp rods, a kind of three‐dimensional (3D), mesh‐like lamellar structured hemp‐based biomass carbon aerogel (CA) was developed by freeze‐drying and subsequent high‐temperature carbonization method. The microstructure, flame resistance, thermal stability, and thermal conductivity of CA were investigated using several analytical techniques, including scanning electron microscopy (SEM), Fourier‐transform infrared spectroscopy (FTIR), X‐ray diffraction (XRD), simulated combustion tests, and thermogravimetric analysis (TG). Optimum formulation yielded at an alkali treatment concentration of 20% and a carbonization temperature of 700°C, CA with a 3D network of reticulated lamellae was obtained. CA exhibited minimal values for thermal conductivity (0.06 W/m K) and thermal diffusion coefficient (0.41 mm2/s), which are indicative of superior insulative properties. Moreover, the material demonstrated remarkable thermal endurance and flame resistance, achieving a char yield of 70.03% when subjected to a temperature of 700°C in an oxidative environment.

Funder

Natural Science Foundation of Shanxi Province

Shanxi Scholarship Council of China

Publisher

Wiley

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