Abstract
Heating a solution of t-butanol in acidified deuterium oxide under slight pressure has yielded 85% per-deuterated t-butanol. At atmospheric pressure normal isobutylene was produced. Isobutylene could not be hydrated in good yield by this method. A number of related alcohols were resistant to exchange by this method, but one of them, 1-methylcyclohexanol, gave nearly complete dehydration without deuterium incorporation.
Publisher
Canadian Science Publishing
Subject
Organic Chemistry,General Chemistry,Catalysis
Cited by
4 articles.
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