Less is more: A simple methyl-TROSY based pulse scheme offers improved sensitivity in applications to high molecular weight complexes-Reference-Cited by-同舟云学术

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Less is more: A simple methyl-TROSY based pulse scheme offers improved sensitivity in applications to high molecular weight complexes

Published:2023-01 Issue: Volume:346 Page:107326
ISSN:1090-7807
Container-title:Journal of Magnetic Resonance
language:en
Short-container-title:Journal of Magnetic Resonance

Author:

Bolik-Coulon Nicolas,Sever Alexander I.M.,Harkness Robert W.,Aramini James M.,Toyama Yuki,Hansen D. Flemming,Kay Lewis E.

Funder

Natural Sciences and Engineering Research Council of Canada

Biotechnology and Biological Sciences Research Council

Uehara Memorial Foundation

Japan Society for the Promotion of Science

Canadian Institutes of Health Research

Publisher

Elsevier BV

Subject

Condensed Matter Physics,Nuclear and High Energy Physics,Biochemistry,Biophysics

Reference38 articles.

1. NMR spectroscopy captures the essential role of dynamics in regulating biomolecular function;Alderson;Cell,2021

2. Biomolecular NMR spectroscopy. Chem. Rev. 122 (2022) 9265–10086.

3. Attenuated T2 relaxation by mutual cancellation of dipole-dipole coupling and chemical shift anisotropy indicates an avenue to NMR structures of very large biological macromolecules in solution;Pervushin;Proc. Natl. Acad. Sci.,1997

4. Cross-correlated relaxation enhanced 1H–13C NMR spectroscopy of methyl groups in very high molecular weight proteins and protein complexes;Tugarinov;J. Am. Chem. Soc.,2003

5. NMR studies of large proteins;Jiang;J. Mol. Biol.,2017

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2. Hyperpolarized nuclear Overhauser enhancement of alanine methyl groups by doubly relayed proton exchange;Journal of Magnetic Resonance;2024-07

3. Sedimentation of large, soluble proteins up to 140 kDa for 1H-detected MAS NMR and 13C DNP NMR – practical aspects;Journal of Biomolecular NMR;2024-06-21

4. Solution-state methyl NMR spectroscopy of large non-deuterated proteins enabled by deep neural networks;Nature Communications;2024-06-13

5. Atomic resolution map of the solvent interactions driving SOD1 unfolding in CAPRIN1 condensates;2024-05-02

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