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Development of a derivatization RP-HPLC method for determination of sulfuryl chloride in chlorosulfonic acid for gefapixant citrate manufacture

  • Published:2022-06 Issue: Volume:215 Page:114752
  • ISSN:0731-7085
  • Container-title:Journal of Pharmaceutical and Biomedical Analysis
  • language:en
  • Short-container-title:Journal of Pharmaceutical and Biomedical Analysis

Author:

Huang Chunli,Song Siqing,Liu Wenjun,Parganiha Priya,Zhuang Ping,Lohani Sachin,Alwedi Embarek,Ren Hong,Bishara Daniel,Chang Hsieh Yao D.

Publisher

Elsevier BV

Subject

Clinical Biochemistry,Spectroscopy,Drug Discovery,Pharmaceutical Science,Analytical Chemistry

Reference18 articles.

1. Development of a green and sustainable manufacturing process for gefapixant citrate (MK-7264) part 1: introduction and process overview;Ren;Org. Process Res. Dev.,2020

2. Chlorosulfuric Acid;Maas,2002

3. Druggable negative allosteric site of P2×3 receptors;Wang;Proc. Natl. Acad. Sci. U. S. .A,2018

4. Development of a green & sustainable manufacturing process for gefapixant citrate (MK-7264) part 5: completion of the API free base via a direct chlorosulfonylation process;Di Maso;Org. Process. Res. Dev.,2020

5. Determination of sulfuryl chloride in thionyl chloride;Marciniak;Pr. Inst. Przemyslu Org.,1971

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